It is, of course, possible
to speed up the operation of the tanks, in which case it would be advisable
to increase the nickel content. However, this would not be practical at present;
there is no point in operating a solution faster than work can be cleaned for
it.
A report in regard to magnesium
sulphate might not be amiss. The advantages noted to the magnesium sulphate
are (1) a whiter, more easily shined plate, and (2) perhaps a contribution to
our freedom from pitting.
For over a year, as a result
of this close control, these solutions have given absolutely no trouble; pitting
and allied troubles are unknown. Since our solution pHs are held practically
constant we have had but little contact with the defects resulting from improper
acidity content. In general it may be said that we prefer a comparatively high
pH. We think that it is an important factor in elimination of pitting, and further,
that the plate resulting is more easily buffed. It may be added here that the
thickness of the average coating applied in our plating room is between .0001
inch and .001 inch. It seems evident that without the check on acidity afforded
by means of pH determinations, close control of all the other factors involved
would be futile, as far as freedom from trouble is concerned. But, were not
the other variables also under control, pH control, however, careful, would
be inadequate.
The writer wishes to acknowledge
indebtedness to Mr. Danz, foreman, Western Clock Co. plating room. He contributed
much in the way of information and advice.
CLEVELAND F. NIXON.
READ AT NEWARK BRANCH BY
MR. HORACE H. SMITH
Platinum Bath
Half ounce platinum dissolved in aqua regia, evaporate until syrupy, add one
pint of water, then add saturated solution of ammonium phosphate until all platinum
is precipitated. Boil until all ammonia is evaporated. Test with red litmus
paper until it no longer turns blue. Then add one ounce phosphate of soda and
one ounce pyrophosphate sodium. Add water to make one quart. Use at 180 degrees
Fahrenheit, 5 to 6 volts.
Platinum No. 2
Dissolve 1.25 dwts. of platinum in aqua regia ( 1 oz. of hydrochloric acid to
3/4 oz. of nitric acid).
Boil and renew the aqua
regia if necessary until the plati-num is dissolved. When all of the platinum
has dissolved, boil down the solution until most of the acid is gone and a brown
syrupy liquid is left. Do NOT allow it to dry out.
Weigh out 12 dwts. of ammonium
phosphate and dissolve it in 2 oz. of boiling water. Pour this solution into
the platinum solution and stir the mixture. (This will destroy the acid remaining
with the platinum and give a thick light yellow mixture of platinum ammonium
phosphate.)
Weigh out 80 dwts. of sodium phosphate crystals and dissolve in 3 oz. of water.
It will be NECESSARY to boil the mixture to dissolve all of the sodium phosphate.
While hot, this solution is poured into the platinum ammonium phosphate, and
the whole mixture boiled down to 4 oz.
(Sodium phosphate can be
bought as the dry salt, or in crystals. If the dry salt is used, weigh out 32
dwts. in place of the 80 dwts. of crystals. Containers of sodium phosphate crystals
are either marked CRYSTALS or Na2HPO4 .12H2O.)
The above solution should
be diluted with 6 or 7 times its volume of water before using.
CHROMIUM PLATING
O. F. Carlson, J. L. Mott Co.,
Trenton, N. J. (Read at Newark Branch)
The following is a description
of methods being pursued in chromium plating plumbing supplies in the J. L.
Mott plant at Trenton, N. J.
The equipment consists of
an iron tank, acid-proof, porcelain enamel-lined, fitted with a hood connected
with an exhaust fan to draw out the fumes, it is also fitted with a lead steam
coil, and another lead pipe with 3/16-inch holes 2 inches apart from compressed
air agitation, the anodes are lead strips 3/4 x 1/2-inch, 5 inches apart, and
bolted and soldered to a heavy brass anode hook fitted with a set screw, so
that a tight and permanent connection can be made with the anode rod.
It is equipped with a 600-amp.
crown rheostat, with voltmeter and ammeter, also quick reading thermometer mounted
on instrument board, with extension hanging in tank.
The solution is composed
as follows:
Chromic acid, 33 oz.
Chromium sulphate, 0.4 oz.
Boracic acid, 1 oz. per gallon.
Current pressure, 7 to 9 volts.
Temperature, 115 to 120 deg. F.
Time of deposit, 6 to 7 minutes.
The current must be turned
on all the time and connection quickly made, as the action of the solution without
the current renders the surface passive.
The most important part
of chromium plating successfully is the method of racking the work; the racks
must be constructed so that the parts can be either screwed or forced tightly
on the arms of the racks, and the hook of the rack fitted with a set screw,
so that a tight connection with the rod can be made; allowance must be made
for plenty of space between the parts, as they cannot be crowded, and we find
that we get the best results by depositing direct on the brass, as giving a
nickel strike does not improve the throwing power and shows a tendency to blister
the nickel.
PITTSBURGH BRANCH
Meeting held Saturday evening, June 4th, in the downtown branch Y. M. C. A.,
with ten members present. The election of delegates to Toledo convention resulted
as follows:
Delegates, Herman Peter, S. E. Hedden, E. S. Corbit. Alternates, Henry Wiesner
and John Corbit. We expect to have at least 12 members going to Toledo from
Pittsburgh, and possibly more, as all present were making plans to attend.
After a social hour, in which all took part, meeting adjourned, to meet Saturday
evening, July 9th, when it is expected that the delegates to Toledo will we
able to give a good account of themselves, as well as the doings of the convention
at Toledo.
S. E. HEDDEN, Secretary.
NEW YORK BRANCH
The May meetings of the New York Branch were well attended. The both meetings
were given over to the nominations and election of officers: The following were
elected for the coming term:
President, Frank MacStocker; vice-president, Arthur Grinham; secretary-treasurer,
Ralph Lignori; recording secretary, Thomas Gardner; sergeant-at-arms, Ben Nadel;
assistant sergeant-at-arms, Charles Hanshalter; librarian, Elias Schorr; trustees,
Fred Hanshalter, William Fisher, Joseph Menges; delegates to the Toledo convention,
Frank MacStocker, George Wilson, Philip Morningstar; alternates, Anthony Knechtel,
Arthur Grinham, William Fisher.
RALPH LIGNORI, Recording Secretary.
ROCHESTER BRANCH
Regular monthly meeting, Rochester Branch, held May 20th, 1927, at the Powers
Hotel.
Mr. J. J. Desmond, chief chemist, North East Electric Co., gave a very interesting
talk on chromium plating. A general discussion followed.
The following officers were elected for the ensuing year: President, Raymond
P. Lopez, vice-president, Charles Griffin, secretary-treasurer, Sylvester P.
Gartland; librarian, Thomas Harper. Delegates to the Fifteenth Annual Convention:
F. C. Mesle, supreme president; R. P. Topez, S. P. Gartland.
We had the pleasure of a visit from our friend, Dr. William Blum, who spoke
at the Chamber of Commerce before the superintendent group on chromium plating.
A number of our plants have installed chromium-plating baths and judging by
the samples on display at our last meeting they are meeting with success.
At our next regular meeting June 17th we will have a report on the number of
members who will attend the convention at Toledo, Ohio. SYLVESTER P. GARTLAND,
Secretary-Treasurer.
CHICAGO BRANCH
Regular monthly meeting and annual smoker of Chicago Branch held June 11th,
1927, at Atlantic Hotel.
Meeting was called to order with President Jacob Hay, presiding and a very large
attendance.
After the regular routine of business, the electing of Mr. Wm. H. Hanson to
active membership and the application of Mr. Elburn L. Fish referred to an investigating
committee, the president called upon Mr. Frank J. Hanlon to act as master of
ceremonies with the assistance of Mr. R. J. Hazucaha as marshall to install
the newly-elected officers which are as follows:
President--Robt. Meyer.
Vice-PresidentR. J. Kelley.
Secretary-Treasurer--Samuel J. C. Trapp, 1127 N. Seventh Ave., Maywood, Ill.
Librarian--R. E. Lewis.
Board of Managers--Cyril Kocom, F. L. Greenwald and Henry Lanz.
The newly-installed president was then presented with the gavel who proceeded
to call upon several of the old-timers and past presidents for a few remarks
of encouragement.
Mr. Jack Geisman was requested to sing a few of his favorite songs which were
enjoyed by all.
Music was furnished by the Benson entertainers who also led in community singing..
Owing to the late hour the question box was held over until next meeting.
The evening was enjoyed by everyone and the harmony and good fellowship shown
bears watching for Chicago Branch to have a banner year.
All together boys, here we go for a steady stride forward.
DAYTON BRANCH
June meeting was well attended and a very lively discussion on chrome plate
seemed to keep the boys guessing as how to plate large flat pieces ranging from
14 to 20 inches square. Seemed to have trouble getting the centers covered but
with all the suggestions offered no doubt someone will bring us something at
our next meeting at any rate quite a few members promised to attend the Toledo
convention to see if they might brush up a bit on the subject; The proposed
structive talk on chrome plating. We were further surprised by Clarence Van
Deran from Mansfield, Ohio, who also gave us a talk Chrome plating in large
production. Both speakers were interesting ad all who attended received considerable
experience, as both of these men know how to put it over. We also had a very
good talk by Mr. Jones from the Westinghouse plant of Mansfield, Ohio, who gave
a very good talk on inspection. Mr. Jones put this over very good, as he is
the chief inspector of the Westinghouse plants and sure knows his job. The speakers
were given a rising vote of thanks. Meeting adjourned at a late hour.
Following is results of election held May 7, 1927:
President, Wm. Hohman; Vice-President, Jacob Zwisler; Secretary Treasurer, R.
G. Suman. Board of Managers: Walter Fraine, Wm. Brandt, H. J. Harter. Delegates
to Convention: Walter Fraine, Clarence Van Deran, R. G. Suman. Alternates: Wm.
Hohman, Ira Van Pelt, H. J. Harter. ROBERT G. SUMAN, Secretary.
CHICAGO BRANCH
Regular monthly meeting Chicago Branch, A. E. S., held May 14 1927, Atlantic
Hotel. The meeting was called to order, with President Jacob Hay presiding,
and a very large attendance.
Mr. H. A. Gilbertson, Chairman of the Booster Committee, reported that the New
York Central Railroad has agreed to put on a special car for the members of
Chicago Branch and their friends who wish to attend the Toledo (Ohio) Convention.
Notices as to the time, etc., have been sent out to the members and manufacturers
to this effect.
Our annual election of officers was held at this meeting. The results were as
follows: President, R. Meyers; Vice-President, Roy Kelley; Secretary-Treasurer,
Samuel Trapp; Librarian, O. E. Servis. These offices were elected by acclamation.
Board of Managers: Cyril Kocour. F. .L. Greenwald, Henry Lanz. Considerable
interest was shown in the election of the Board of Managers, the first returns
resulting in a tie, and the second returns were very closely contested.
Delegates to Newark Convention: F. J. Hanlon, Jacob Hay, R. Meyers. Alternates:
O. E. Servis, P. L. Greenwald, Samuel Trapp.
Mr. Erwin Sohn of the Pittsburg Branch; also Mr. Blitz of Milwaukee Branch and
E. V. Allen were visiting with us.
The balance of the evening
was given over to the question box.
Question 1: My cadmium plating water stains. How can I prevent it ?
Answer: Work should be dipped in whale oil soap, rinsed in cold water, dry in
oven. Selicate of soda was also suggested.
Question 2: What addition do you make to an old silver solution to make it plate
a pearl white?
Answer: Reduce cyanide or add metal. High cyanide content was thought to cause
it to be off color.
Question 3: How can you increase throwing power of chromium plating solution
?
Answer: By adding an iron salt was suggested.
ROBERT MEYERS, Secretary-Treasurer.